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This laboratory manual of Pharmaceutical Inorganic Chemistry has been carefully designed in accordance with the latest PCI syllabus for B. Pharma First Semester students. It aims to serve as a complete, reliable, and student-friendly guide for developing practical skills and conceptual clarity in the laboratory. The manual presents experiments in a simple, structured and easy-to-follow format, ensuring that students can confidently perform procedures while understanding the scientific principles behind them. Each experiment is supported with well-organized tables, clear diagrams, and illustrative charts that transform complex concepts into visual learning experiences. Special emphasis has been placed on accuracy, safety and systematic observation, which are essential components of pharmaceutical laboratory practice. This manual is not just a record book, but a companion that guides students step by step, from preparation to result interpretation. If used sincerely, this manual will be sufficient for mastering the prescribed practical syllabus, eliminating the need for additional laboratory references. It is our sincere hope that this work inspires curiosity, builds confidence, and lays a strong foundation for future pharmaceutical studies and professional excellence. Ms. Amrita Yadav Mr. Raj Kumar Vishwakarma Mr. Sahil Akhtar Ms. Prakriti Maurya Mr. Pawan Verma